Glycosylation intermediates studied using low temperature 1H- and 19F-DOSY NMR: new insight into the activation of trichloroacetimidates

Publikation: Bidrag til tidsskrift › Letter › Forskning › fagfællebedømt

Standard

Glycosylation intermediates studied using low temperature 1H- and 19F-DOSY NMR : new insight into the activation of trichloroacetimidates. / Qiao, Yan; Ge, Wenzhi; Jia, Lingyu; Hou, Xianglin; Wang, Yingxiong; Pedersen, Christian Marcus.

I: Chemical Communications, Bind 52, Nr. 76, 2016, s. 11418-11421.

Publikation: Bidrag til tidsskrift › Letter › Forskning › fagfællebedømt

Harvard

Qiao, Y, Ge, W, Jia, L, Hou, X, Wang, Y & Pedersen, CM 2016, 'Glycosylation intermediates studied using low temperature 1H- and 19F-DOSY NMR: new insight into the activation of trichloroacetimidates', Chemical Communications, bind 52, nr. 76, s. 11418-11421. https://doi.org/10.1039/c6cc05272j

APA

Qiao, Y., Ge, W., Jia, L., Hou, X., Wang, Y., & Pedersen, C. M. (2016). Glycosylation intermediates studied using low temperature 1H- and 19F-DOSY NMR: new insight into the activation of trichloroacetimidates. Chemical Communications, 52(76), 11418-11421. https://doi.org/10.1039/c6cc05272j

Vancouver

Qiao Y, Ge W, Jia L, Hou X, Wang Y, Pedersen CM. Glycosylation intermediates studied using low temperature 1H- and 19F-DOSY NMR: new insight into the activation of trichloroacetimidates. Chemical Communications. 2016;52(76):11418-11421. https://doi.org/10.1039/c6cc05272j

Author

Qiao, Yan ; Ge, Wenzhi ; Jia, Lingyu ; Hou, Xianglin ; Wang, Yingxiong ; Pedersen, Christian Marcus. / Glycosylation intermediates studied using low temperature 1H- and 19F-DOSY NMR : new insight into the activation of trichloroacetimidates. I: Chemical Communications. 2016 ; Bind 52, Nr. 76. s. 11418-11421.

Bibtex

@article{f2ae91899b9248039ab448cfd3265d74,
title = "Glycosylation intermediates studied using low temperature 1H- and 19F-DOSY NMR: new insight into the activation of trichloroacetimidates",
abstract = "Low temperature 1H- and 19F-DOSY have been used for analyzing reactive intermediates in glycosylation reactions, where a glycosyl trichloroacetimidate donor has been activated using different catalysts. The DOSY protocols have been optimized for low temperature experiments and provided new insight into acid catalyzed glycosylation chemistry. From the study a new glycosylation intermediate was characterized.",
author = "Yan Qiao and Wenzhi Ge and Lingyu Jia and Xianglin Hou and Yingxiong Wang and Pedersen, {Christian Marcus}",
year = "2016",
doi = "10.1039/c6cc05272j",
language = "English",
volume = "52",
pages = "11418--11421",
journal = "Chemical Communications",
issn = "1359-7345",
publisher = "Royal Society of Chemistry",
number = "76",

}

RIS

TY - JOUR

T1 - Glycosylation intermediates studied using low temperature 1H- and 19F-DOSY NMR

T2 - new insight into the activation of trichloroacetimidates

AU - Qiao, Yan

AU - Ge, Wenzhi

AU - Jia, Lingyu

AU - Hou, Xianglin

AU - Wang, Yingxiong

AU - Pedersen, Christian Marcus

PY - 2016

Y1 - 2016

N2 - Low temperature 1H- and 19F-DOSY have been used for analyzing reactive intermediates in glycosylation reactions, where a glycosyl trichloroacetimidate donor has been activated using different catalysts. The DOSY protocols have been optimized for low temperature experiments and provided new insight into acid catalyzed glycosylation chemistry. From the study a new glycosylation intermediate was characterized.

AB - Low temperature 1H- and 19F-DOSY have been used for analyzing reactive intermediates in glycosylation reactions, where a glycosyl trichloroacetimidate donor has been activated using different catalysts. The DOSY protocols have been optimized for low temperature experiments and provided new insight into acid catalyzed glycosylation chemistry. From the study a new glycosylation intermediate was characterized.

U2 - 10.1039/c6cc05272j

DO - 10.1039/c6cc05272j

M3 - Letter

C2 - 27722642

AN - SCOPUS:84987889390

VL - 52

SP - 11418

EP - 11421

JO - Chemical Communications

JF - Chemical Communications

SN - 1359-7345

IS - 76

ER -

ID: 169729177